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Descrição
Tired of jars, breaking glass, and spilled and spoiled staining reagent, we designed a universal dipping chamber for thin-layer chromatography!
Three predefined models are provided:
Synthesis Style: medium sized for 10x10 cm plates, with a spout, a lid, and a pedestal to keep it from falling over.
HPTLC: for 20x10 cm plates with a spout, a lid, and a shell to tightly close the lid and store the reagent in the freezer (a sealing ring is recommended!)
Micro: if you like using really small plate and need really just very little reagent; with a pedestal and a lid.
If you want to make your own custom chamber, use the "dipping_chamber_parameters.scad" to set the dimensions and add or remove options. Presets for the three provided chambers are provided in the "dipping_chamber_parameters_Synthesis Style/HPTLC/Micro.scad" file.
After adjusting the settings in the parameters-file, use "dipping_chamber.scad" to prepare an stl for the dipping chamber, "dipping_chamber_lid.scad" for a lid, and "dipping_chamber_shell.scad" for a shell to hold the lid in place. Please take a moment before printing to check if the models make sense, as OpenSCAD does not prevent you from entering silly parameters.
Please take a moment after printing to check if the chamber is tight, because printing PP is not easy.
Interested in a more chemical perspective? There is a publication at [https://doi.org/10.1016/j.talanta.2020.121072](https://doi.org/10.1016/j.talanta.2020.121072)
Print instructions
Printing conditions:
Printer: Prusa i3 MK3S (MMU2S installed but not required)
Material: PP
Resolution: 0.3 mm
Infill: Gyroid 5%
Brim: 20 mm
!Changes in Layers and perimeters!
Solid layers, top: 5
Avoid crossing perimeters
Detect thin walls
Detect brindging perimeters
Preparation of the printing surface:
The printing surface was prepared by carefully applying clear PP adhesive tape onto the preheated smooth PEI sheet.
Dipping Chambers for Thin Layer Chromatography
Publicado em 22 de abr de 2020
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